Synthesis, Crystal Structure, Thermal Behavior and Optical Properties of An Organic Light-Emitting Diode Compound

Volume 5, Issue 4, August 2020     |     PP. 71-78      |     PDF (424 K)    |     Pub. Date: September 25, 2020
DOI:    212 Downloads     3001 Views  

Author(s)

Yuanyuan Sun, Xi'an Manareco New Material Co., Ltd., Affiliated 71#, 2nd Jinye Rd, Gaoxin District, Xi'an, Shanxi, People’s Republic of China.

Abstract
The title compound, C53H36N5, was synthesized and characterized by IR and single-crystal X-ray diffraction analysis. The structure analysis indicates that the compound crystallizes in the triclinic space group P-1 and employs C–H‧‧‧π and π‧‧‧π weak interactions to stabilize the structure. The compound exhibits good thermal stability, which can maintain the skeleton until 400 °C. It can be used for green organic light-emitting diode devices exhibiting good performance.

Keywords
9-(3'-(4,6-diphenyl-1,3,5-triazin-2-yl)-[1,1'-biphenyl]-3-yl)-14-phenyl-9,14-dihydrodibenzo[2,3:6,7]azepino[4,5-b]indole; Crystalline structure; Organic light-emitting diode

Cite this paper
Yuanyuan Sun, Synthesis, Crystal Structure, Thermal Behavior and Optical Properties of An Organic Light-Emitting Diode Compound , SCIREA Journal of Chemistry. Volume 5, Issue 4, August 2020 | PP. 71-78.

References

[ 1 ] Huang, M.-H.; Chang, C.-P. A comparative study on detecting research fronts in the organic light-emitting diode (OLED) field using bibliographic coupling and co-citation. Scientometrics. 2015, 102, 2041-2057.
[ 2 ] Yeom, J.-M.; Jung, H.-J.; Choi, S.-Y.; Lee, D. S.; Lim, S.-R. Environmental Effects of the Technology Transition from Liquid–Crystal Display (LCD) to Organic Light-Emitting Diode (OLED) Display from an E-Waste Management Perspective. Int. J. Environ. Res. 2018, 12, 479-488.
[ 3 ] Andrew C. Grimsdale, K. L. C., Rainer E. Martin, Pawel G. Jokisz, and Andrew B. Holmes. Synthesis of Light-Emitting Conjugated Polymers for Applications in Electroluminescent Devices. Chem. Rev. 2009, 109, 897-1091.
[ 4 ] Salunke, J. K.; Wong, F. L.; Feron, K.; Manzhos, S.; Lo, M. F.; Shinde, D.; Patil, A.; Lee, C. S.; Roy, V. A. L.; Sonar, P.; Wadgaonkar, P. P. Phenothiazine and carbazole substituted pyrene based electroluminescent organic semiconductors for OLED devices. J. Mater. Chem. C. 2016, 4, 1009-1018.
[ 5 ] Mohammad, A.-T.; Yeap, G.-Y.; Osman, H. Synthesis, characterization and theoretical study of a new liquid crystal compound with an oxazepine core. J. Mol. Struct. 2015, 1087, 88-96.
[ 6 ] Sheldrick, G. M. A short history of SHELX. Acta Crystallogr A. 2008, 64, 112-122.
[ 7 ] Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr C Struct Chem. 2015, 71, 3-8.
[ 8 ] Effendy; Junk, P. C.; Kepert, C. J.; Louis, L. M.; Morien, T. C.; Skelton, B. W.; White, A. H. The Structural Systematics of Protonation of Some Important Nitrogen-base Ligands. III. Some (Univalent) Anion Salts of some Hindered Unidentate Nitrogen Bases. Z. Anorg. Allg. Chem. 2006, 632, 1312-1325.
[ 9 ] B. Ahrens, P. G. J., A. K. Fischer. Gold(I) Complexes with Amine Ligands, 4[°] The Role of N–H···Cl Hydrogen Bonds in Gold(I) Complexes with Aliphatic Amine Ligands. Eur. J. Inorg. Chem. 1999, 1103-1110.
[ 10 ] R. Tacke, R. B., C. Burschka, S. Dragota, M. Penka, I. Richter. Spirocyclic Zwitterionic ì5Si-Silicates with Two Bidentate Ligands Derived from r-Amino Acids or r-Hydroxycarboxylic Acids: Synthesis, Structure, and Stereodynamics. J. Am. Chem. Soc. 2004, 126, 14493-14505.